2,2',4,4'-Tetrahydroxybenzophenone → HCID 135401076, compound

HRID 1294885Notes

Reaction equation

HRID 1294885 reaction equation
O[C:2]1[CH:17]=[C:16]([OH:18])[CH:15]=[CH:14][C:3]=1[C:4]([C:6]1[CH:11]=[CH:10][C:9]([OH:12])=[CH:8][C:7]=1[OH:13])=O.C([O-])(=O)C.[Na+].Cl.[CH3:25][O:26][C:27]1[CH:32]=[CH:31][C:30]([NH:33][NH2:34])=[CH:29][CH:28]=1>>[OH:18][C:16]1[CH:17]=[C:2]2[C:3]([C:4]([C:6]3[CH:11]=[CH:10][C:9]([OH:12])=[CH:8][C:7]=3[OH:13])=[N:34][N:33]2[C:30]2[CH:31]=[CH:32][C:27]([O:26][CH3:25])=[CH:28][CH:29]=2)=[CH:14][CH:15]=1

Participants

4

Reactant 3

HCID 85712,2',4,4'-TetrahydroxybenzophenoneHCID 517045Sodium AcetateHCID 27239044-Methoxyphenylhydrazine hydrochloride

Product 1

HCID 135401076HCID 135401076, compoundYield 7.5%

Procedure

Prepared according to Method B from 2,2′,4,4′-tetrahydroxybenzophenone (0.123 g, 0.5 mmol), sodium acetate (0.041 g, 0.5 mmol) and 4-methoxyphenylhydrazine hydrochloride (0.087 g, 0.5 mmol) to give 0.013 g of product as a tan solid

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-46abf3aa77294288a696287ddabfcf98
Source dataset
uspto-grants-2007_07
Patent number
US07241791B2

Reaction notes

Loading…