Cyclohexene → HCID 178423643, compound

HRID 1294915Notes

Reaction equation

HRID 1294915 reaction equation
C[O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[C:17]3[C:12](=[C:13]([CH3:18])[CH:14]=[CH:15][CH:16]=3)[NH:11][N:10]=2)=[CH:5][CH:4]=1.B(Br)(Br)Br.C1CCCCC=1>>[CH3:18][C:13]1[CH:14]=[CH:15][CH:16]=[C:17]2[C:12]=1[NH:11][N:10]=[C:9]2[C:6]1[CH:5]=[CH:4][C:3]([OH:2])=[CH:8][CH:7]=1

Participants

4

Reactant 3

HCID 8079CyclohexeneHCID 25134Boron tribromideHCID 178489133HCID 178489133, compound

Product 1

HCID 178423643HCID 178423643, compoundYield 74.3%

Procedure

Prepared according to Method D step C from 3-(4-methoxyphenyl)-7-methyl-1H-indazole (0.10 g, 0.42 mmol), boron tribromide (0.159 mL, 1.68 mmol) and 0.5 mL of cyclohexene to give the product (0.070 g) as an off-white solid.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-2d6f187872f249bebc30b796c4126bd0
Source dataset
uspto-grants-2007_07
Patent number
US07241791B2

Reaction notes

Loading…