HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Iodopentane → 3-(4-methoxyphenyl)-7-methyl-1-pentyl-1H-indazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Iodopentane | HCID 12335 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 178489133 | HCID 178489133 | — |
| Product | 3-(4-methoxyphenyl)-7-methyl-1-pentyl-1H-indazole | HCID 68883395 | 34% |
Reaction Steps
Prepared according to Method D step B from 3-(4-methoxyphenyl)-7-methyl-1H-indazole (0.23 g, 1.0 mmol), sodium hydride (60% in oil, 0.048 g, 1.2 mmol) and 1-iodopentane (0.26 mL, 2.0 mmol) to give the title compound (0.105 g) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241791B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-432383fd7cea40fc912a1c75948b0680 |
| Source note | uspto-grants-2007_07 |