Cyclohexene → HCID 135527000, compound

HRID 1294922Notes

Reaction equation

HRID 1294922 reaction equation
C[O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[N:10]([CH2:19][CH2:20][CH3:21])[N:11]=[C:12]3[C:17]=2[CH:16]=[CH:15][CH:14]=[C:13]3[CH3:18])=[CH:5][CH:4]=1.B(Br)(Br)Br.C1CCCCC=1>>[CH3:18][C:13]1[C:12]2[C:17](=[C:9]([C:6]3[CH:5]=[CH:4][C:3]([OH:2])=[CH:8][CH:7]=3)[N:10]([CH2:19][CH2:20][CH3:21])[N:11]=2)[CH:16]=[CH:15][CH:14]=1

Participants

4

Reactant 3

HCID 8079CyclohexeneHCID 25134Boron tribromideHCID 68883555HCID 68883555, compound

Product 1

HCID 135527000HCID 135527000, compoundYield 52.6%

Procedure

Prepared according to Method D step C from 3-(4-methoxyphenyl)-7-methyl-2-propyl-2H-indazole (0.014 g, 0.05 mmol), boron tribromide (0.050 mL, 1.0 mmol) and 0.2 mL of cyclohexene to give the product (0.007 g).

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-96f02d10969a46e5ba28ea4cd1868dca
Source dataset
uspto-grants-2007_07
Patent number
US07241791B2

Reaction notes

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