Cyclohexene → HCID 68885402, compound

HRID 1294926Notes

Reaction equation

HRID 1294926 reaction equation
[CH:1]([N:4]1[CH:12]([C:13]2[CH:18]=[CH:17][C:16]([O:19]C)=[CH:15][CH:14]=2)[C:11]2[C:6](=[C:7]([CH3:21])[CH:8]=[CH:9][CH:10]=2)[NH:5]1)([CH3:3])[CH3:2].B(Br)(Br)Br.C1CCCCC=1>>[CH:1]([N:4]1[CH:12]([C:13]2[CH:14]=[CH:15][C:16]([OH:19])=[CH:17][CH:18]=2)[C:11]2[C:6](=[C:7]([CH3:21])[CH:8]=[CH:9][CH:10]=2)[NH:5]1)([CH3:3])[CH3:2]

Participants

4

Reactant 3

HCID 8079CyclohexeneHCID 25134Boron tribromideHCID 68883658HCID 68883658, compound

Product 1

HCID 68885402HCID 68885402, compoundYield 74.5%

Procedure

Prepared according to Method D step C from 2-isopropyl-3-(4-methoxyphenyl)-7-methyl-1H-indazole (0.010 g, 0.035 mmol), boron tribromide (0.05 mL, 0.5 mmol) and 0.2 mL of cyclohexene to give the product (0.007 g).

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-5ea442ecb30249e08f5efce9054950ee
Source dataset
uspto-grants-2007_07
Patent number
US07241791B2

Reaction notes

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