Cyclohexene → HCID 68882126, compound

HRID 1294937Notes

Reaction equation

HRID 1294937 reaction equation
[Cl:1][C:2]1[C:10]2[C:6](=[C:7]([C:14]3[CH:19]=[CH:18][C:17]([O:20]C)=[CH:16][CH:15]=3)[N:8]([CH:11]([CH3:13])[CH3:12])[N:9]=2)[CH:5]=[CH:4][CH:3]=1.B(Br)(Br)Br.C1CCCCC=1>>[Cl:1][C:2]1[CH:3]=[CH:4][CH:5]=[C:6]2[C:10]=1[NH:9][N:8]([CH:11]([CH3:13])[CH3:12])[CH:7]2[C:14]1[CH:15]=[CH:16][C:17]([OH:20])=[CH:18][CH:19]=1

Participants

4

Reactant 3

HCID 8079CyclohexeneHCID 25134Boron tribromideHCID 68884529HCID 68884529, compound

Product 1

HCID 68882126HCID 68882126, compoundYield 41.6%

Procedure

Prepared according to Method D step C from 7-chloro-2-isopropyl-3-(4-methoxyphenyl)-2H-indazole (0.016 g, 0.05 mmol), boron tribromide (0.050 mL, 0.5 mmol) and 0.2 mL of cyclohexene to give the product (0.006 g).

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-922cecee0ef1440fb20a55a18723e7f5
Source dataset
uspto-grants-2007_07
Patent number
US07241791B2

Reaction notes

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