Cyclohexene → HCID 135518191, compound

HRID 1294947Notes

Reaction equation

HRID 1294947 reaction equation
[Cl:1][C:2]1[C:10]2[C:6](=[C:7]([C:16]3[CH:21]=[CH:20][C:19]([O:22]C)=[CH:18][CH:17]=3)[N:8]([CH:11]3[CH2:15][CH2:14][CH2:13][CH2:12]3)[N:9]=2)[C:5](C)=[CH:4][CH:3]=1.B(Br)(Br)Br.C1CCCCC=1>>[Cl:1][C:2]1[C:10]2[C:6](=[C:7]([C:16]3[CH:17]=[CH:18][C:19]([OH:22])=[CH:20][CH:21]=3)[N:8]([CH:11]3[CH2:15][CH2:14][CH2:13][CH2:12]3)[N:9]=2)[CH:5]=[CH:4][CH:3]=1

Participants

4

Reactant 3

HCID 8079CyclohexeneHCID 25134Boron tribromideHCID 68884097HCID 68884097, compound

Product 1

HCID 135518191HCID 135518191, compoundYield 106.6%

Procedure

Prepared according to Method D step C from 7-chloro-2-cyclopentyl-3-(4-methoxyphenyl)-methyl-2H-indazole (0.004 g, 0.012 mmol), boron tribromide (0.10 mL, 1.05 mmol) and 0.3 mL of cyclohexene to give the product (0.004 g).

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-c286077a04e84bec951732828572a321
Source dataset
uspto-grants-2007_07
Patent number
US07241791B2

Reaction notes

Loading…