HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → 7-fluoro-3-(4-methoxyphenyl)-1-propyl-1H-indazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 1-Iodopropane | HCID 33643 | — |
| Reactant | HCID 178489142 | HCID 178489142 | — |
| Product | 7-fluoro-3-(4-methoxyphenyl)-1-propyl-1H-indazole | HCID 68884303 | 52.1% |
Reaction Steps
Prepared according to Method D step B from 7-fluoro-3-(4-methoxyphenyl)-1H-indazole (0.121 g, 0.5 mmol), sodium hydride (60% in oil, 0.024 g, 0.6 mmol) and 1-iodopropane (0.096 mL, 1.0 mmol) to give the title compound (0.074 g) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241791B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-f4ee1e4799ec4034bce34a6c37608b5f |
| Source note | uspto-grants-2007_07 |