HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexane → HCID 15665590, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexane | HCID 8058 | — |
| Reactant | Piperidin-4-ol | HCID 79341 | — |
| Reactant | HCID 86746988 | HCID 86746988 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 15665590 | HCID 15665590 | 101.7% |
Reaction Steps
10.0 g of 3-butynylphenyl carbonate and 5.8 g of 4-hydroxypiperidine were heated in a solvent-free condition at 100° C. of 30 minutes. After completion of the reaction, silica gel column chromatography (elution solvent: hexane:ethyl acetate=1:1-1:2) was used for purification to obtain 10.6 g of the intended compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05468740 |
| Source dataset | uspto-grants-1995_11 |
| ORD ID | ord-ba1fc660cc4449ab902d1555888191ac |
| Source note | uspto-grants-1995_11 |