Cyclohexene → HCID 135516773, compound

HRID 1294961Notes

Reaction equation

HRID 1294961 reaction equation
[CH2:1]([N:4]1[C:12]([C:13]2[CH:18]=[CH:17][C:16]([O:19]C)=[CH:15][CH:14]=2)=[C:11]2[C:6]([C:7]([C:21]([F:24])([F:23])[F:22])=[CH:8][CH:9]=[CH:10]2)=[N:5]1)[CH:2]=[CH2:3].B(Br)(Br)Br.C1CCCCC=1>>[CH2:1]([N:4]1[C:12]([C:13]2[CH:18]=[CH:17][C:16]([OH:19])=[CH:15][CH:14]=2)=[C:11]2[C:6]([C:7]([C:21]([F:24])([F:23])[F:22])=[CH:8][CH:9]=[CH:10]2)=[N:5]1)[CH:2]=[CH2:3]

Participants

4

Reactant 3

HCID 8079CyclohexeneHCID 25134Boron tribromideHCID 68882876HCID 68882876, compound

Product 1

HCID 135516773HCID 135516773, compoundYield 110%

Procedure

Prepared according to Method D step C from 2-allyl-3-(4-methoxyphenyl)-7-trifluoromethyl-2H-indazole (0.007 g, 0.02 mmol), boron tribromide (0.10 mL, 1.05 mmol) and 0.3 mL of cyclohexene to give the product (0.007 g).

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-5681d4786e8644d6be17d90bc3914f89
Source dataset
uspto-grants-2007_07
Patent number
US07241791B2

Reaction notes

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