Cyclohexene → HCID 135492419, compound

HRID 1294989Notes

Reaction equation

HRID 1294989 reaction equation
[CH2:1]([N:4]1[C:12]([C:13]2[CH:18]=[CH:17][C:16]([O:19]C)=[CH:15][C:14]=2[CH3:21])=[C:11]2[C:6]([C:7]([Cl:22])=[CH:8][CH:9]=[CH:10]2)=[N:5]1)[CH:2]=[CH2:3].B(Br)(Br)Br.C1CCCCC=1>>[CH2:1]([N:4]1[C:12]([C:13]2[CH:18]=[CH:17][C:16]([OH:19])=[CH:15][C:14]=2[CH3:21])=[C:11]2[C:6]([C:7]([Cl:22])=[CH:8][CH:9]=[CH:10]2)=[N:5]1)[CH:2]=[CH2:3]

Participants

4

Reactant 3

HCID 8079CyclohexeneHCID 25134Boron tribromideHCID 68882833HCID 68882833, compound

Product 1

HCID 135492419HCID 135492419, compoundYield 108.8%

Procedure

Prepared according to Method D step C from 2-allyl-7-chloro-3-(4-methoxy-2-methylphenyl)-2H-indazole (0.068 g, 0.2 mmol), boron tribromide (0.20 mL, 2.10 mmol) and 1.0 mL of cyclohexene to give the product (0.065 g) as a white solid.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-dff80848c1ac4c7da093de2e105bcf23
Source dataset
uspto-grants-2007_07
Patent number
US07241791B2

Reaction notes

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