HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromocyclopentane → 1-cyclopentyl-3-(2,4-dimethoxyphenyl)-7-fluoro-1H-indazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromocyclopentane | HCID 8728 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 3-(2,4-dimethoxyphenyl)-7-fluoro-1H-indazole | HCID 178489145 | — |
| Product | 1-cyclopentyl-3-(2,4-dimethoxyphenyl)-7-fluoro-1H-indazole | HCID 68882324 | 125% |
Reaction Steps
Prepared according to Method D step B from 3-(2,4-dimethoxyphenyl)-7-fluoro-1H-indazole (0.150 g, 0.55 mmol), sodium hydride (60% in oil, 0.058 g, 0.66 mmol) and cyclopentyl bromide (0.214 mL, 2.0 mmol) to give the title compound (0.234 g) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241791B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-54ddf5aa11284b19b60beaf381ab4dac |
| Source note | uspto-grants-2007_07 |