HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexene → 4-(7-fluoro-2-isobutyl-2H-indazol-3-yl)benzene-1,3-diol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexene | HCID 8079 | — |
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | 3-(2,4-dimethoxyphenyl)-7-fluoro-2-isobutyl-2H-indazole | HCID 68884123 | — |
| Product | 4-(7-fluoro-2-isobutyl-2H-indazol-3-yl)benzene-1,3-diol | HCID 136358467 | 79.9% |
Reaction Steps
Prepared according to Method D step C from 3-(2,4-dimethoxyphenyl)-7-fluoro-2-isobutyl-2H-indazole (0.036 g, 0.1 mmol), boron tribromide (0.083 mL, 0.9 mmol) and 1.0 mL of cyclohexene to give the product (0.024 g) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241791B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-b2bef97f64374285aa6e26fb5d6b2bd4 |
| Source note | uspto-grants-2007_07 |