HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexene → 4-(2-allyl-7-fluoro-2H-indazol-3-yl)benzene-1,3-diol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexene | HCID 8079 | — |
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | 2-allyl-3-(2,4-dimethoxyphenyl)-7-fluoro-2H-indazole | HCID 68882446 | — |
| Product | 4-(2-allyl-7-fluoro-2H-indazol-3-yl)benzene-1,3-diol | HCID 136358469 | 40.5% |
Reaction Steps
Prepared according to Method D step C from 2-allyl-3-(2,4-dimethoxyphenyl)-7-fluoro-2H-indazole (0.057 g, 0.2 mmol), boron tribromide (0.150 mL, 1.6 mmol) and 1.0 mL of cyclohexene to give the product (0.023 g) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241791B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-98098d1e788f4394b7e21af7a8320944 |
| Source note | uspto-grants-2007_07 |