HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromopropane → HCID 68884157, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromopropane | HCID 7840 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 178489138 | HCID 178489138 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 68884157 | HCID 68884157 | — |
Reaction Steps
Prepared according to Method D Step B from 7-chloro-3-(3-chloro-4-methoxyphenyl)-1H-indazole (1.0 g, 3.4 mmol), sodium hydride (0.15 g, 60% in oil) in DMF followed by propyl bromide (0.4 mL). The title compound was obtained as an oil (0.94 g, 2.8 mmol, 82%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241791B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-a70b5bd3e61d4b989a0e095ffe6175d0 |
| Source note | uspto-grants-2007_07 |