HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pivaloyl chloride → HCID 68884169, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pivaloyl chloride | HCID 62493 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | 4-(1-cyclopentyl-7-fluoro-1H-indazol-3-yl)phenol | HCID 135524867 | — |
| Product | HCID 68884169 | HCID 68884169 | 81.5% |
Reaction Steps
Prepared according to Method E from 4-(1-cyclopentyl-7-fluoro-1H-indazol-3-yl)phenol (0.30 g, 1.0 mmol), pivaloyl chloride (0.148 mL, 1.2 mmol) and N,N-diisopropylethyl-amine (0.21 mL, 1.2 mmol) to give 0.31 g of the title compound as a white solid, mp 105° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241791B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-137c1f4c54a247158790cb244fc1fd84 |
| Source note | uspto-grants-2007_07 |