HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → 2-Chloro-N-ethyl-5-hydroxybenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | 2-Chloro-5-hydroxybenzoic acid | HCID 458210 | — |
| Product | 2-Chloro-N-ethyl-5-hydroxybenzamide | HCID 58907486 | — |
Reaction Steps
The title compound was prepared from 2-chloro-5-hydroxybenzoic acid and ethylamine, using a method similar to that used for preparation 52, as a colourless solid. 1HNMR (400 MHz, CDCl3) δ: 1.22 (3H, t), 3.42–3.49 (2H, m), 6.48–6.52 (1H, m), 6.80 (1H, dd), 7.13 (1H, d), 7.38 (1H, d); LRMS ESI m/z 200 [M+H]+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241810B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-1887cb4f412d407db3003ab77cc1f53a |
| Source note | uspto-grants-2007_07 |