HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenemethanamine, 3,4-dimethyl- → 2-(3-Bromophenyl)-N-(3,4-dimethylbenzyl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenemethanamine, 3,4-dimethyl- | HCID 66888 | — |
| Reactant | (3-Bromophenyl)acetic acid | HCID 74653 | — |
| Product | 2-(3-Bromophenyl)-N-(3,4-dimethylbenzyl)acetamide | HCID 58907514 | 93% |
Reaction Steps
The title compound was prepared from 3,4-dimethylbenzylamine and 3-bromophenylacetic acid, using a method similar to that of preparation 27, as a white solid in 93% yield. 1H NMR (400 MHz, CDCl3) δ: 2.20 (6H, s), 3.50 (2H, s), 4.30 (2H, d), 5.80 (1H, brs), 7.60–7.80 (7H, m); LRMS ESI 332 [M]+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241810B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-d73a4913b8e84f7686bf2952dfa5cbaf |
| Source note | uspto-grants-2007_07 |