HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butanal → 56249-61-7
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butanal | HCID 261 | — |
| Reactant | Benzylamine | HCID 7504 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 56249-61-7 | HCID 4555911 | — |
Reaction Steps
This material is a known compound prepared in the standard fashion. To about 100 mL of toluene was added 28 mL of butyraldehyde, 34 mL of benzylamine, and several grams of 3A molecular sieves. The mixture became warm and turbid after standing for a few minutes. After standing for several hours the mixture was colorless and transparent. The imine product was isolated by distillation under vacuum and characterized by NMR spectroscopy.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241839B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-975dd027af1d4246842a1aa172023b42 |
| Source note | uspto-grants-2007_07 |