3-Chloro-2-butanone → HCID 69115169, compound

HRID 1295528Notes

Reaction equation

[CH3:1][NH:2][C:3](=[S:6])[NH:4][NH2:5].[Cl:7][CH:8]([CH3:12])[C:9](=O)[CH3:10]>>[ClH:7].[CH3:1][N:2]1[C:9]([CH3:10])=[C:8]([CH3:12])[S:6][C:3]1=[N:4][NH2:5]

Participants

Reactant 2

HCID 200263-Chloro-2-butanone

HCID 2723853N-Methylhydrazinecarbothioamide

Product 1

HCID 69115169HCID 69115169, compound

Procedure

3,4,5-Trimethyl-2(3H)thiazolone hydrazone hydrochloride was prepared from 4-methyl-3-thiosemicarbazide and 3-chloro-2-butanone by a method similar to that used in Example (1a).

Sources & evidence

ORD record: ord-078402a8669e4632a6dbc84e577f0023
Source dataset: uspto-grants-2007_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07244278B2

Reaction notes

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