Isobutyraldehyde → HCID 23105941, compound

HRID 1295604Notes

Reaction equation

HRID 1295604 reaction equation
Br[C:2]1[CH:3]=[CH:4][C:5]([Cl:12])=[C:6]([C:8]([F:11])([F:10])[F:9])[CH:7]=1.[CH:13](=[O:17])[CH:14]([CH3:16])[CH3:15]>>[Cl:12][C:5]1[CH:4]=[CH:3][C:2]([CH:13]([OH:17])[CH:14]([CH3:16])[CH3:15])=[CH:7][C:6]=1[C:8]([F:11])([F:10])[F:9]

Participants

3

Reactant 2

HCID 6561IsobutyraldehydeHCID 679594-Bromo-2-chloro-alpha,alpha,alpha-trifluorotoluene

Product 1

HCID 23105941HCID 23105941, compound

Procedure

Prepared analogously to the method described for Example 1a) from 2.3 mL (15 mmol) of 5-bromo-2-chlorobenzotrifluoride and 1.3 mL (14 mmol) isobutyraldehyde. Yellow oil. Yield: 2.0 g (53%).

Workup

  1. customPrepared analogously to the method

Sources & evidence

ORD record
ord-079dca0ff64d4f6d8e44536f90488d3e
Source dataset
uspto-grants-2007_07
Patent number
US07244728B2

Reaction notes

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