HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Acetyl-6-aminoindoline → HCID 9904166, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Acetyl-6-aminoindoline | HCID 258564 | — |
| Reactant | HCID 10131256 | HCID 10131256 | — |
| Solvent | Isopropanol methylene chloride | HCID 21966342 | — |
| Product | HCID 9904166 | HCID 9904166 | 4% |
Reaction Steps
Example 10 was prepared as a white solid in 4% yield from Compound A of Example 1 and 1-acetyl-6-aminoindoline as described for Compound B of Example 1, using 10% isopropanol/methylene chloride for extraction, and with purification by chromatography on silica gel with ethyl acetate. (M+H)+=294.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07244733B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-5471bdf9b0244fc68e5b4528699591fd |
| Source note | uspto-grants-2007_07 |