HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 15125753, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | (E)-methyl 3-methoxy-2-(2-[3-carboxyphenoxy]phenyl)propenoate | HCID 15125752 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 15125753 | HCID 15125753 | — |
Reaction Steps
The carboxylic acid from the previous stage (0.33 g) stirred in dry THF (10 ml) was treated with oxalyl chloride (0.11 ml) and one drop of dry DMF. The reaction mixture was stirred for 45 minutes, stood overnight and then evaporated to give crude (E)-methyl 3-methoxy-2-(2-[3-chlorocarbonylphenoxy]phenyl)propenoate as an orange-yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05468857 |
| Source dataset | uspto-grants-1995_11 |
| ORD ID | ord-6d48a705a43f4fcd85bb80bb24537931 |
| Source note | uspto-grants-1995_11 |