Formaldehyde → HCID 22504868, compound
Reaction equation
COC(=O)COC1C=C(OC)C(SCCCNC2C=CC(C3C=CC=CC=3)=CN=2)=CC=1C.C=O.C[O:36][C:37](=[O:68])[CH2:38][O:39][C:40]1[CH:45]=[C:44]([O:46][CH3:47])[C:43]([S:48][CH2:49][CH2:50][CH2:51][N:52]([CH2:65]C)[C:53]2[CH:58]=[CH:57][C:56]([C:59]3[CH:64]=[CH:63][CH:62]=[CH:61][CH:60]=3)=[CH:55][N:54]=2)=[CH:42][C:41]=1[CH3:67]>>[CH3:47][O:46][C:44]1[C:43]([S:48][CH2:49][CH2:50][CH2:51][N:52]([CH3:65])[C:53]2[CH:58]=[CH:57][C:56]([C:59]3[CH:60]=[CH:61][CH:62]=[CH:63][CH:64]=3)=[CH:55][N:54]=2)=[CH:42][C:41]([CH3:67])=[C:40]([CH:45]=1)[O:39][CH2:38][C:37]([OH:68])=[O:36]Participants
4
Procedure
Compound 64B was reacted with paraformaldehyde in a manner analogous to Compound 64C to give the title product. MS m/z 467 (M+1).
Sources & evidence
- ORD record
- ord-74c4d38d65cd4f37bd32c624abd63cb6
- Source dataset
- uspto-grants-2007_07
- Patent number
- US07244763B2
Reaction notes
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