HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetaldehyde → 5-Bromo-N-ethylpyridin-2-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetaldehyde | HCID 177 | — |
| Reactant | 2-Amino-5-bromopyridine | HCID 70622 | — |
| Reactant | (4-{3-[Ethyl-(5-phenyl-pyridin-2-yl)-amino]-propylsulfanyl}-5-methoxy-2-methyl-phenoxy)-acetic acid methyl ester | HCID 20770817 | — |
| Product | 5-Bromo-N-ethylpyridin-2-amine | HCID 22504916 | — |
Reaction Steps
5-Bromo-pyridin-2-ylamine and acetaldehyde were treated under the conditions of Compound 64C to give the intermediate (5-bromo-pyridin-2-yl)-ethyl-amine. This was then reacted with Compound 64A to give the title product. MS m/z 481 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07244763B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-a00fc9c0810446b28450bf7b7d7a2c1d |
| Source note | uspto-grants-2007_07 |