4-Chlorophenylboronic acid → HCID 11461257, compound

HRID 1296523Notes

Reaction equation

HRID 1296523 reaction equation
[NH2:1][C:2]1[CH:3]=[CH:4][C:5]2[N:10]([CH3:11])[C:9](=[O:12])[O:8][C:7]([CH3:14])([CH3:13])[C:6]=2[CH:15]=1.[Cl:16][C:17]1[CH:22]=[CH:21][C:20](B(O)O)=[CH:19][CH:18]=1>>[Cl:16][C:17]1[CH:22]=[CH:21][C:20]([NH:1][C:2]2[CH:3]=[CH:4][C:5]3[N:10]([CH3:11])[C:9](=[O:12])[O:8][C:7]([CH3:13])([CH3:14])[C:6]=3[CH:15]=2)=[CH:19][CH:18]=1

Participants

3

Reactant 2

HCID 742994-Chlorophenylboronic acidHCID 69215309HCID 69215309, compound

Product 1

HCID 11461257HCID 11461257, compound

Procedure

Prepared from 6-amino-1,4,4-trimethyl-1,4-dihydro-2H-3,1-benzoxazin-2-one and 4-chlorophenyl boronic acid according to the coupling procedure described in example 1. MS (ESI) m/z [M+H]+ (317/319); MS (ESI) m/z [M−H]−(315/317); Anal. calcd for C17H17ClN2O2: C, 64.46; H, 5.41; N, 8.84. Found: C, 63.40; H, 5.46; N, 7.97.

Sources & evidence

ORD record
ord-c45ece2a0b26412489dbc3ec75648c35
Source dataset
uspto-grants-2007_07
Patent number
US07247625B2

Reaction notes

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