2-Chlorophenylboronic acid → HCID 11738612, compound

HRID 1296524Notes

Reaction equation

HRID 1296524 reaction equation
[NH2:1][C:2]1[CH:3]=[CH:4][C:5]2[N:10]([CH3:11])[C:9](=[O:12])[O:8][C:7]([CH3:14])([CH3:13])[C:6]=2[CH:15]=1.[Cl:16][C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=1B(O)O>>[Cl:16][C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=1[NH:1][C:2]1[CH:3]=[CH:4][C:5]2[N:10]([CH3:11])[C:9](=[O:12])[O:8][C:7]([CH3:13])([CH3:14])[C:6]=2[CH:15]=1

Participants

3

Reactant 2

HCID 27343222-Chlorophenylboronic acidHCID 69215309HCID 69215309, compound

Product 1

HCID 11738612HCID 11738612, compound

Procedure

Prepared from 6-amino-1,4,4-trimethyl-1,4-dihydro-2H-3,1-benzoxazin-2-one and 2-chlorophenyl boronic acid according to the coupling procedure described in example 1. MS (ESI) m/z [M+H]+ (317/319); MS (ESI) m/z [M−H]− (315/317); Anal. calcd for C17H17ClN2O2: C, 64.46; H, 5.41; N8.84. Found: C, 64.42; H, 5.29; N8.76.

Sources & evidence

ORD record
ord-dfd7f527d6294798816307e8f32bd65b
Source dataset
uspto-grants-2007_07
Patent number
US07247625B2

Reaction notes

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