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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 129671Generated: October 29, 2026

HCID 14852535, compound → HCID 19372199, compound

https://huagongshe.com/reaction/129671

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 14852535HCID 14852535—
CatalystPalladiumHCID 23938—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 19372199HCID 19372199100.5%

Reaction Steps

Into a reactor there are introduced 3 g (10 mmoles) of methyl 3-(1-adamantyl)-4-vinylbenzoate, 270 mg of palladium on charcoal (5%) and 50 ml of dioxan. Hydrogenation is effected at ambient temperature and under a pressure of 4 bars for 4 hours. The catalyst is filtered and the filtrate is evaporated. 3 g (100% yield) of the expected product in the form of a colorless oil are recovered.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05468897
Source datasetuspto-grants-1995_11
ORD IDord-ff710f9dd62a447e8f7fed48b0abb079
Source noteuspto-grants-1995_11