HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14852535, compound → HCID 19372199, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14852535 | HCID 14852535 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 19372199 | HCID 19372199 | 100.5% |
Reaction Steps
Into a reactor there are introduced 3 g (10 mmoles) of methyl 3-(1-adamantyl)-4-vinylbenzoate, 270 mg of palladium on charcoal (5%) and 50 ml of dioxan. Hydrogenation is effected at ambient temperature and under a pressure of 4 bars for 4 hours. The catalyst is filtered and the filtrate is evaporated. 3 g (100% yield) of the expected product in the form of a colorless oil are recovered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05468897 |
| Source dataset | uspto-grants-1995_11 |
| ORD ID | ord-ff710f9dd62a447e8f7fed48b0abb079 |
| Source note | uspto-grants-1995_11 |