HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlororesorcinol → HCID 58913623, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlororesorcinol | HCID 1731 | — |
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | (3-Methoxyphenyl)acetic acid | HCID 15719 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Product | HCID 58913623 | HCID 58913623 | — |
Reaction Steps
This compounds was synthesised in the same manner as described above. 4-Chlororesorcinol (1.74 g, 12 mmol), 3-methoxyphenylacetic acid (2.0 g, 12 mmol), BF3Et2O (5 ml), PCl5 (3.75 g, 18 mmol), DMF (15 ml and 10 ml). 6-Chloro-7-hydroxy-3-(3-methoxy-phenyl)-chromen-4-one precipitated out as a white solid (1.6 g, 44%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247734B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-7319f4ae4f1e4c6a87595142bab64272 |
| Source note | uspto-grants-2007_07 |