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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1296906Generated: October 29, 2026

Hydrazine hydrate (1:1) → HCID 178511052, compound

https://huagongshe.com/reaction/1296906

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrazine hydrate (1:1)HCID 24654—
ReactantHCID 58913568HCID 58913568—
ProductHCID 178511052HCID 17851105271.6%

Reaction Steps

This compounds was synthesised in the same manner as described above. 4-[4-(6-Chloro-7-hydroxy-4-oxo-4H-chromen-3-yl)-phenoxy]-butyronitrile (0.12 g, 0.34 mmol), Hydrazine hydrate (5 ml). The precipitate formed on quenching was filtered to give 4-{4-[3-(5-Chloro-2,4-dihydroxy-phenyl)-1H-pyrazol-4-yl]-phenoxy}-butyronitrile as a white solid (0.09 g, 71.6%); Rf 0.6 ethyl acetate/hexane (70/30)].

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07247734B2
Source datasetuspto-grants-2007_07
ORD IDord-7feca21117d2473c9792699b8e71dab0
Source noteuspto-grants-2007_07