HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylresorcinol → 4-chloro-2-methyl-benzene-1,3-diol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylresorcinol | HCID 11843 | — |
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 4-chloro-2-methyl-benzene-1,3-diol | HCID 11205924 | — |
Reaction Steps
To a solution of 2-methyl resorcinol (1 eq) in MeCN (5 ml) was added N-chlorosuccinimide (1 eq) and refluxed under nitrogen overnight. The yellow solution was concentrated in vacuo and purified by flash chromatography to give 4-chloro-2-methyl-benzene-1,3-diol as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07247734B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-f3c5f8a7f317437cbd1645ce25c08484 |
| Source note | uspto-grants-2007_07 |