N-(4-Bromobutyl)phthalimide → HCID 54420745, compound

HRID 129741Notes

Reaction equation

HRID 129741 reaction equation
[CH2:1]1[C@H:6]2[C:7]3[CH:19]=[CH:18][CH:17]=[CH:16][C:8]=3[CH2:9][C:10]3[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=3[N:5]2[CH2:4][CH2:3][NH:2]1.Br[CH2:21][CH2:22][CH2:23][CH2:24][N:25]1[C:29](=[O:30])[C:28]2=[CH:31][CH:32]=[CH:33][CH:34]=[C:27]2[C:26]1=[O:35]>>[C:26]1(=[O:35])[N:25]([CH2:24][CH2:23][CH2:22][CH2:21][N:2]2[CH2:3][CH2:4][N:5]3[C:11]4[CH:12]=[CH:13][CH:14]=[CH:15][C:10]=4[CH2:9][C:8]4[CH:16]=[CH:17][CH:18]=[CH:19][C:7]=4[C@@H:6]3[CH2:1]2)[C:29](=[O:30])[C:28]2=[CH:31][CH:32]=[CH:33][CH:34]=[C:27]12

Participants

3

Reactant 2

HCID 93575N-(4-Bromobutyl)phthalimideHCID 153935136315-26-9

Product 1

HCID 54420745HCID 54420745, compound

Procedure

Following a procedure similar to that described in Preparation 14(a), but using (14bR)-1,2,3,4,10,14b-hexahydrodibenzo[c,f]pyrazino[1,2-a]azepine and N-(4-bromobutyl)phthalimide, the title compound was obtained in a quantitative yield.

Sources & evidence

ORD record
ord-19f886769f9a47c68f6246da4bfa26e3
Source dataset
uspto-grants-1995_11
Patent number
US05470851

Reaction notes

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