N-3-Bromopropylphthalimide → HCID 19370259, compound

HRID 129768Notes

Reaction equation

HRID 129768 reaction equation
Br[CH2:2][CH2:3][CH2:4][N:5]1[C:9](=[O:10])[C:8]2=[CH:11][CH:12]=[CH:13][CH:14]=[C:7]2[C:6]1=[O:15].[S:16]1[CH:20]=[CH:19][CH:18]=[C:17]1[C:21](=[C:28]1[CH2:33][CH2:32][NH:31][CH2:30][CH2:29]1)[C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1>>[S:16]1[CH:20]=[CH:19][CH:18]=[C:17]1[C:21](=[C:28]1[CH2:33][CH2:32][N:31]([CH2:2][CH2:3][CH2:4][N:5]2[C:9](=[O:10])[C:8]3=[CH:11][CH:12]=[CH:13][CH:14]=[C:7]3[C:6]2=[O:15])[CH2:30][CH2:29]1)[C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1

Participants

3

Reactant 2

HCID 21611N-3-BromopropylphthalimideHCID 19370322HCID 19370322, compound

Product 1

HCID 19370259HCID 19370259, compoundYield 84%

Procedure

The title compound was prepared in a yield of 84% in a similar manner to that described in Preparation 1' by reacting N-(3-bromopropyl)phthalimide and 4-[α-(2-thienyl)benzylidene]piperidine.

Workup

  1. customdescribed in Preparation 1'

Sources & evidence

ORD record
ord-c507513b3124456da0ea06900650f9b0
Source dataset
uspto-grants-1995_11
Patent number
US05470851

Reaction notes

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