HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Acetate → 6-(4-Oxo-2-thioxo-thiazolidin-5-ylidenemethyl)-4-pyridin-3-yl-quinoline-3-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | Rhodanine | HCID 1201546 | — |
| Reactant | 6-Formyl-4-pyridin-3-yl-quinoline-3-carbonitrile | HCID 58585838 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 6-(4-Oxo-2-thioxo-thiazolidin-5-ylidenemethyl)-4-pyridin-3-yl-quinoline-3-carbonitrile | HCID 76823843 | — |
Reaction Steps
Similar procedure as described in example 61j was used, starting from 6-formyl-4-pyridin-3-yl-quinoline-3-carbonitrile (example 63c), rhodanine, sodium acetate, and acetic acid to give 6-(4-oxo-2-thioxo-thiazolidin-5-ylidenemethyl)-4-pyridin-3-yl-quinoline-3-carbonitrile. LC-MS m/e 375 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07250515B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-63945e74924a459a81227e876e7fe444 |
| Source note | uspto-grants-2007_07 |