HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 68825937, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 86602497 | HCID 86602497 | — |
| Product | HCID 68825937 | HCID 68825937 | — |
Reaction Steps
Similar procedure as described in example 41b was used, starting from 1-butoxy-7-(4-oxo-2-thioxo-thiazolidin-5-ylidenemethyl)-naphthalene-2-carbonitrile (example 79c), iodomethane, and DIEA (diisopropylethylamine) in acetonitrile to give 4-butoxy-6-(2-methylsulfanyl-4-oxo-4H-thiazol-5-ylidenemethyl)-quinoline-3-carbonitrile. LC-MS m/e 384 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07250515B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-d6a7d0af82bb49609466907bd7a4e3a9 |
| Source note | uspto-grants-2007_07 |