HCID 178441737, compound → 1H-Imidazole-4-carboxaldehyde, 5-bromo-2-butyl-

Participants

Reaction Conditions

Reaction Steps

4.37 g of the product of Step A were introduced into 130 ml of dioxane and then 16.32 g of manganese dioxide were added with stirring. The mixture was heated to approximately 100° C. for about 2 hours, then filtered. The filtrate was rinsed with dioxane and evaporated to obtain 3.72 g of the expected product melting at 113° C.

Provenance & Evidence