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HRID129904

反应详情

EQUATION

反应方程式

HRID 129904 的结构方程式

REACTANTS

反应物

2
结构：O=[N+]([O-])[O-].O=[N+]([O-])[O-].[Zn+2]
HCID24518

Zinc nitrate

N2O6Zn

结构：CN(C)Cc1cc(CN(C)C)c([O-])c(CN(C)C)c1.[Na+]
HCID23711567

Sodium 2,4,6-tris(dimethylaminomethyl)phenolate

C15H26N3NaO

PRODUCTS

生成物

1
结构：CN(C)Cc1cc(CN(C)C)c([O-])c(CN(C)C)c1.CN(C)Cc1cc(CN(C)C)c([O-])c(CN(C)C)c1.[Zn+2]
HCID67805255

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCO
溶剂HCID263

1-Butanol

C4H10O

PROCEDURE

实验过程

5.7 g (0.02 mol) of sodium 2,4,6-tris(dimethylaminomethyl)phenolate (preparation see Example 19) and 17.9 g of 1-butanol are placed in a 100 ml round-bottomed flask having a magnetic stirrer, and then 3.0 g (0.01 mol) of zinc nitrate are added. The solution is stirred for 45 minutes, and then the precipitated sodium nitrate is filtered off. A clear, dark-brown 25% accelerator solution of zinc bis(2,4,6-tris(dimethylaminomethyl)phenolate) in 1-butanol is obtained.

WORKUP

后处理

  1. filtrationthe precipitated sodium nitrate is filtered off