Methylhydrazine → 1-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl 2-Methylhydrazinecarboxylate

HRID 129967Notes

Reaction equation

HRID 129967 reaction equation
Cl[C:2]([O:4][CH:5]1[CH2:10][C:9]([CH3:12])([CH3:11])[N:8]([O:13][CH3:14])[C:7]([CH3:16])([CH3:15])[CH2:6]1)=[O:3].[CH3:17][NH:18][NH2:19]>CO>[CH3:17][NH:18][NH:19][C:2]([O:4][CH:5]1[CH2:10][C:9]([CH3:12])([CH3:11])[N:8]([O:13][CH3:14])[C:7]([CH3:16])([CH3:15])[CH2:6]1)=[O:3]

Participants

4

Reactant 2

HCID 6061MethylhydrazineHCID 540353651-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl Cloroformate

Product 1

HCID 544690901-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl 2-Methylhydrazinecarboxylate

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The title compound is prepared by reacting the compound of Example 27 (1 mole) with methylhydrazine (1.1 mole) in methanol.

Sources & evidence

ORD record
ord-55321efcdb8d475c90b1230e4cb34c1a
Source dataset
uspto-grants-1995_11
Patent number
US05470980

Reaction notes

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