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HRID130297

反应详情

EQUATION

反应方程式

HRID 130297 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)c1ccc2ccccc2c1
HCID7122

2'-Acetonaphthone

C12H10O

结构：CCOC(=O)C(F)(F)C(F)(F)F
HCID67928

Ethyl perfluoropropionate

C5H5F5O2

PRODUCTS

生成物

1
结构：O=C(CC(=O)C(F)(F)C(F)(F)F)c1ccc2ccccc2c1
HCID15787980

4,4,5,5,5-Pentafluoro-1-(naphthalen-2-yl)pentane-1,3-dione

C15H9F5O2

PROCEDURE

实验过程

The compound was synthesized according to example 1 using 2-acetylnaphthalene and ethyl pentafluoropropionate as starting materials. The product was crystallized from petroleum ether. 1H NMR (CDCl3): 6.79 (s, 1 H); 7.57-7.67 (m, 2H); 7.90 (bd, 1 H); 7.94-7.95 (m, 2H); 7.99 (bd, 1H); 8.53 (s, 1 H). IR (film): 1602 (C═O); 1201 (C—F).

WORKUP

后处理

  1. customThe compound was synthesized
  2. customThe product was crystallized from petroleum ether