Hydrochloric Acid → HCID 59007048, compound

Participants

Reaction Steps

A mixture of product from Step 3 (883 mg, 3 mmol) in ethanol (40 ml) containing concentrated hydrochloric acid (2 ml) was heated at reflux for 15 hours. After cooling, the mixture was purified using an SCX ion exchange cartridge (Varian bond-elute) eluting with methanol and then 2M ammonia in methanol. The appropriate basic fractions were reduced in vacuo to afford the title compound (D18). MS (ES+) m/e 254 [M+H]+.

Provenance & Evidence