4-Iodobenzenesulfonyl chloride → N-[5-Bromo-2-(methyloxy)phenyl]-4-iodobenzenesulfonamide

HRID 130469Notes

Reaction equation

HRID 130469 reaction equation
[Br:1][C:2]1[CH:3]=[CH:4][C:5]([O:9][CH3:10])=[C:6]([CH:8]=1)[NH2:7].[I:11][C:12]1[CH:17]=[CH:16][C:15]([S:18](Cl)(=[O:20])=[O:19])=[CH:14][CH:13]=1>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([O:9][CH3:10])=[C:6]([NH:7][S:18]([C:15]2[CH:16]=[CH:17][C:12]([I:11])=[CH:13][CH:14]=2)(=[O:20])=[O:19])[CH:8]=1

Participants

3

Reactant 2

HCID 73994-Iodobenzenesulfonyl chlorideHCID 35853285-Bromo-2-methoxyaniline

Product 1

HCID 47310943N-[5-Bromo-2-(methyloxy)phenyl]-4-iodobenzenesulfonamide

Procedure

The title compound was prepared from 5-bromo-2-(methyloxy)aniline and 4-iodobenzenesulfonyl chloride using a similar method to that described for Examples 82-100 (E82-E100). MS (ES−) 466/468 [M−H]−.

Sources & evidence

ORD record
ord-d66309d841d249a68aaf803967a9ab73
Source dataset
uspto-grants-2008_06
Patent number
US07381728B2

Reaction notes

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