돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 130895생성일: 2026년 10월 25일

(5,6-Dichloropyridin-3-yl)methanol → 5,6-Dichloropyridine-3-carbaldehyde

https://huagongshe.com/reaction/130895

반응식

참여 물질

역할이름HCID투입량
반응물(5,6-Dichloropyridin-3-yl)methanolHCID 21882961—
촉매HCID 178418406HCID 178418406—
용매DichloromethaneHCID 6344—
생성물5,6-Dichloropyridine-3-carbaldehydeHCID 1153565448%

반응 단계

Combine (5,6-dichloro-pyridin-3-yl)-methanol (3.05 g, 17.11 mmol) and manganese dioxide (37.2 g, 427.9 mmol) in CH2Cl2 (25 mL). Stir the reaction mixture at rt overnight. Filter the reaction mixture through Celite® washing with CH2Cl2 (2×10 mL). Concentrate the filtrate and dry under vacuum to provide the title compound (1.44 g, 48%).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07381719B2
출처 데이터셋uspto-grants-2008_06
ORD IDord-1eedb8e0688043248b814c4e9ca0649d
출처 메모uspto-grants-2008_06