HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 178501119, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 178511262 | HCID 178511262 | — |
| Product | HCID 178501119 | HCID 178501119 | — |
Reaction Steps
To a suspension of trans-4-(aminomethyl)cyclohexanecarboxylic acid (6.29 g) in methanol (32 mL) is added dropwise thionyl chloride (6 mL) under ice-cooling and the mixture is stirred at room temperature overnight. The reaction mixture is concentrated in vacuo to give methyl trans-4-(aminomethyl)cyclohexanecarboxylate hydrochloride (8.69 g). MS (APCI) m/z: 172 [M+H]+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07384952B2 |
| Source dataset | uspto-grants-2008_06 |
| ORD ID | ord-d06a4d57df154cb8ab292fd1cedafbb1 |
| Source note | uspto-grants-2008_06 |