HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 86601487, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | N-Hydroxyphthalimide | HCID 10665 | — |
| Reactant | HCID 86597620 | HCID 86597620 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86601487 | HCID 86601487 | — |
Reaction Steps
A mixture of N-hydroxypthalimide (5.3 g), [(2S)-2-methyloxiran-2-yl]methyl 3-nitrobenzenesulfonate (5.9 g) and triethylamine (10.6 ml) in dichloromethane (15 ml) was stirred under nitrogen at ambient temperature for 24 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07384951B2 |
| Source dataset | uspto-grants-2008_06 |
| ORD ID | ord-1345bfbccb634503b7c4e7da8a8b4131 |
| Source note | uspto-grants-2008_06 |