HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Acetamidobenzylamine → HCID 10225262, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Acetamidobenzylamine | HCID 2760946 | — |
| Reactant | 4-[2-methyl-5-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl]benzoic Acid | HCID 11220119 | — |
| Product | HCID 10225262 | HCID 10225262 | — |
Reaction Steps
N-(3-Acetylaminobenzyl)-2′-methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1′-biphenyl-4-carboxamide was prepared from 2′-methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1′-biphenyl-4-carboxylic acid and N-(3-aminomethylphenyl)acetamide using method H. NMR; δH [2H6]—DMSO 9.92,(1H, s), 9.15,(1H, t), 8.01,(2H, d), 7.89,(1H, dd), 7.77,(1H, d), 7.52,(5H, m), 7.23,(1H, t), 6.99,(1H, d), 4.47,(2H, d), 2.56,(3H, s), 2.32,(3H, s), 2.01,(3H, s). LCMS; retention time 2.95 min, MH+ 441.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07384963B2 |
| Source dataset | uspto-grants-2008_06 |
| ORD ID | ord-0929a6c11e1e4064bfa295ce1f832f09 |
| Source note | uspto-grants-2008_06 |