HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzylamine → HCID 10158653, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzylamine | HCID 75452 | — |
| Reactant | 4-[2-methyl-5-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl]benzoic Acid | HCID 11220119 | — |
| Product | HCID 10158653 | HCID 10158653 | — |
Reaction Steps
N-(4-Methoxybenzyl)-2′-methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1′-biphenyl-4-carboxamide was prepared from 2′-methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1′-biphenyl-4-carboxylic acid and 4-methoxybenzylamine using method H. NMR; δH [2H6]—DMSO 9.07,(1H, t), 7.98,(2H, d), 7.89,(1H, dd), 7.76,(1H, d), 7.55-7.50,(3H, m), 7.26,(2H, d), 6.89,(2H, d), 4.43,(2H, d), 3.72,(3H, s), 2.56,(3H, s), 2.31,(3H, s). LCMS; retention time 3.24 min, MH+ 414.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07384963B2 |
| Source dataset | uspto-grants-2008_06 |
| ORD ID | ord-1030bd24d44b4ab385feb883de682e0a |
| Source note | uspto-grants-2008_06 |