HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Phenoxyphenyl)methanamine → HCID 10116392, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Phenoxyphenyl)methanamine | HCID 2760343 | — |
| Reactant | 4-[2-methyl-5-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl]benzoic Acid | HCID 11220119 | — |
| Product | HCID 10116392 | HCID 10116392 | — |
Reaction Steps
2′-Methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-N-(4phenoxybenzyl)-1,1′-biphenyl-4-carboxamide was prepared from 2′-methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1′-biphenyl-4-carboxylic acid and 4-phenoxybenzylamine using method N. NMR; δH [2H6]—DMSO 9.15,(1H, t), 8.00,(2H, d), 7.89,(1H, dd), 7.76,(1H, d), 7.53,(3H, m), 7.37,(4H, m), 7.11,(1H, m), 7.01-6.96,(4H, m), 4.49,(2H, d), 2.56,(3H, s), 2.31,(3H, s). LCMS; retention time 3.76 min, MH+ 476.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07384963B2 |
| Source dataset | uspto-grants-2008_06 |
| ORD ID | ord-422b1135f8934aaaa8be568fb0ae4cf5 |
| Source note | uspto-grants-2008_06 |