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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 131710Generated: November 1, 2026

2-Methoxybenzylamine → HCID 10223476, compound

https://huagongshe.com/reaction/131710

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-MethoxybenzylamineHCID 81292—
Reactant4-[2-methyl-5-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl]benzoic AcidHCID 11220119—
ProductHCID 10223476HCID 10223476—

Reaction Steps

N-(2-Methoxybenzyl)-2′-methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1′-biphenyl-4-carboxamide was prepared from 2′-methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1′-biphenyl-4-carboxylic acid and 2-methoxybenzylamine using method N. NMR; δH [2H6]—DMSO 8.95,(1H, t), 8.02,(2H, d), 7.90,(1H, dd), 7.77,(1H, d), 7.56-7.51,(3H, m), 7.26-7.19,(2H, m), 7.00,(1H, d), 6.91,(1H, t), 4.48,(2H, d), 3.83,(3H, s), 2.56,(3H, s), 2.32,(3H, s). LCMS; retention time 3.41 min, MH+ 414.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07384963B2
Source datasetuspto-grants-2008_06
ORD IDord-a786c61b27804154943b5bffaa91ae9b
Source noteuspto-grants-2008_06