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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 131711Generated: October 26, 2026

2-Methylbenzylamine → HCID 10222443, compound

https://huagongshe.com/reaction/131711

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-MethylbenzylamineHCID 6993—
Reactant4-[2-methyl-5-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl]benzoic AcidHCID 11220119—
ProductHCID 10222443HCID 10222443—

Reaction Steps

2′-Methyl-N-(2-methylbenzyl)-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1′-biphenyl-4-carboxamide was prepared from 2′-methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1′-biphenyl-4-carboxylic acid and 2-methylbenzylamine using method N. NMR; δH [2H6]—DMSO 9.01,(1H, t), 8.01,(2H, d), 7.90,(1H, dd), 7.77,(1H, d), 7.56-7.51,(3H, m), 7.26,(1H, m), 7.18-7.15,(3H, m), 4.48,(2H, d), 2.56,(3H, s), 2.33,(3H, s), 2.31,(3H, s). LCMS; retention time 3.47 min, MH+ 398.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07384963B2
Source datasetuspto-grants-2008_06
ORD IDord-43b17ebee4a1443a9c5882ce4c721488
Source noteuspto-grants-2008_06