4-[2-methyl-5-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl]benzoic Acid → HCID 69221749, compound

HRID 131715Notes

Reaction equation

HRID 131715 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[O:9][C:10]([CH3:13])=[N:11][N:12]=2)=[CH:4][C:3]=1[C:14]1[CH:19]=[CH:18][C:17]([C:20](O)=[O:21])=[CH:16][CH:15]=1.[NH2:23][C:24]1[CH:25]=[CH:26][C:27]([CH3:33])=[C:28]([CH:32]=1)[C:29]([NH2:31])=[O:30]>>[NH2:31][C:29]([C:28]1[CH:32]=[C:24]([NH:23][C:20]([C:17]2[CH:18]=[CH:19][C:14]([C:3]3[CH:4]=[C:5]([C:8]4[O:9][C:10]([CH3:13])=[N:11][N:12]=4)[CH:6]=[CH:7][C:2]=3[CH3:1])=[CH:15][CH:16]=2)=[O:21])[CH:25]=[CH:26][C:27]=1[CH3:33])=[O:30]

Participants

3

Reactant 2

HCID 112201194-[2-methyl-5-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl]benzoic AcidHCID 201446085-Amino-2-methylbenzamide

Product 1

HCID 69221749HCID 69221749, compound

Procedure

N-(3-Aminocarbonyl-4-methylphenyl)-2′-methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1′-biphenyl-4-carboxamide was prepared from 2′-methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1′-biphenyl-4-carboxylic acid and 5-amino-2-methylbenzamide using method I. LCMS; retention time 3.00 min, MH+ 427.

Sources & evidence

ORD record
ord-1bd6c591ad9244689ed2e3083e932bc0
Source dataset
uspto-grants-2008_06
Patent number
US07384963B2

Reaction notes

Loading…